The odour sample is collected in a bag, which is
sealed in a pressurised sample holder. The sample is mixed with
odourfree air in custom designed venturi gas jets without passing
through a flow measurement device. The dilution ratios are adjusted
by a series of needle valves controlled by the digital precision
motion controller with ±0.0001 revolution accuracy. The
diluted odour sample is released via one of two sniffing cups
(another cup contains only odourfree air). In succession, each
member of a panel of six human observers compares the odour of
the two cups without knowing which cup has the diluted odour sample.
The panellists are required to select the cup from which the odour
is presented and to nominate the confidence level of their selection
(guessing, inkling, or certainty). The olfactometer prepares the
next dilution step in ascending concentration level (or descending
dilution ratios). The above procedures are then repeated until
all panellists detect an odour with the confident level of certainty.
The odour concentration is then calculated using the panellists’
responses over the range of dilution settings. There are four
operational modes:
Odour concentrations for environmental samples
Odour concentration is the odour strength expressed
in terms of the number of times the sample is diluted to reach
its odour threshold. At the start of the measurement, determining
the presentation series is of paramount importance to exclude
the possibility of a bias due to the operator’s preference
in choosing the concentration range. The intelligent auto-range
feature allows the optimum starting step to be selected based
on the panellists’ responses. If more than 50% of panellists
record certainty and correct (C&C) responses at the first
dilution step, the current responses are discharged and the first
dilution step is restarted at a new starting step. If necessary,
the process is repeated. Otherwise, the next dilution step is
prepared. The first series is completed when all panellists record
C&C responses. A fresh starting step for the next series is
then calculated according to the result of the first series. The
testing is repeated until all panellists record C&C responses.
Furthermore, a statistical analysis of the two series is performed
to see if two means have a significant difference. If so, a third
series will be added and the results will only be based on the
two series which show no significant difference.
Odour concentrations for reference gases
The European CEN standard requires a reference
gas (such as n-butanol at 60 ppm) to be presented at each panel
session. The results are used to monitor the performance of the
laboratory and individual panellists’ performances. In this
mode, many other reference gases can also be added and their odour
thresholds are determined.
Odour intensity
Odour intensity is the perceived psychophysical
strength of an odour above its odour threshold. Typically, odour
intensity doubles if chemical concentration triples.
The objective of the odour intensity measurement
is to experimentally determine the relationship (Weber-Fechner).
Normally, five dilution steps and a blank are presented randomly.
The minimum dilution step is the level just above its odour concentration.
The panellists sniff the diluted odour from the left cup and select
one of seven odour intensity levels: no odour, very weak, weak,
distinct, strong, very strong and extremely strong. As a result,
the regression between odour intensity levels and the dilution
ratios can be determined.
Ambient odour Intensity index
Using the odour intensity levels mentioned above,
the ambient odours are presented to the panellists. Should the
averaged response to the ambient odour be greater than the distinct
level, it is regarded that the sample has an odour. The results
can be used to solve odour complaints and determine the odour
dispersion patterns.